In this paper, the preparation methods and effect factors of zinc carbohydrazide perchlorate (II) (GTX) are discussed systematically. The best technique parameters of every factor are determined through optimization experiments. Then the optimal technique is acquired, which makes the yield increase to above 80% and crystal forms well. Its explosive properties were tested by friction sensitivities, impact sensitivities and DSC thermal analysis.
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张志刚,张建国,张同来,等.新型起爆药GTX的制备工艺与性能研究[J].含能材料, 2001, 9(2):49-52. ZHANG Zhi-gang, ZHANG Jian-guo, ZHANG Tong-lai, et al. Preparation Technique and Explosive Properties of [Zn(CHZ)3](ClO4)2[J]. Chinese Journal of Energetic Materials, 2001, 9(2):49-52.