The acetylation of 3,4-diaminofurazan (DAF) was studied in this paper. By the reaction of DAF with chloroacetyl chloride and bromoacetyl bromide respectively, the substituted acetyl furazano derivatives were obtained. Then 3-amino-4-(azidoacetamido)furazan was obtained as an high nitrogen content furazano energetic derivative by treating these two intermediates with sodium azide.
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李战雄,唐松青,刘金涛,等.3-氨基4-(叠氮乙酰胺基)呋咱合成[J].含能材料, 2002, 10(3):112-113. LI Zhan-xiong, TANG Song-qing, LIU Jin-tao, et al. Synthesis of 3-Amino-4-(azidoacetamido)Furazan[J]. Chinese Journal of Energetic Materials, 2002, 10(3):112-113.