Isopropyl nitrate is prepared by nitrating isopropanol with nitric acid at 100℃ in the presence of urea and ammonium nitrate. The yield of isopropyl nitrate can be obtained over 85% under the optimum reaction conditions. The purity of isopropyl nitrate can be over 98% based on the analysis of gas chromatography.
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奚美玒.硝酸异丙酯制备工艺研究[J].含能材料, 1998, 6(2):70-72. Xi Mei-hong. A STUDY ON PREPARATION TECHNOLOGY OF ISOPROPYL NITRATE[J]. Chinese Journal of Energetic Materials, 1998, 6(2):70-72.