Study on Synthesis of 1,1-Diamino-2,2-Dinitroethylene
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Low temperature nitration of 2-methylimidazole gave intermediates, which were aminated to form 1,1-diamino-2,2-dinitroethylene .The synthesis route in literature was magnified properly and reaction conditions were optimized. The overall yield was 14.9%.The structure of DADE was characterized by IR, MS, NMR and elemental analysis.
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蔡华强,郁卫飞,田野,等.1,1-二氨基-2,2-二硝基乙烯的合成研究[J].含能材料,2003,11(1):1-3. CAI Hua-qiang, YU Wei-fei, TIAN Ye, et al. Study on Synthesis of 1,1-Diamino-2,2-Dinitroethylene[J]. Chinese Journal of Energetic Materials,2003,11(1):1-3.